K Number
K120652
Date Cleared
2012-10-12

(224 days)

Product Code
Regulation Number
880.2800
Reference & Predicate Devices
Predicate For
N/A
AI/MLSaMDIVD (In Vitro Diagnostic)TherapeuticDiagnosticis PCCP AuthorizedThirdpartyExpeditedreview
Intended Use

The RAPICIDE OPA-28 Test Strip is a chemical indicator for use in determining whether the concentration of ortho-phthalaldehyde, the active ingredient in RAPICIDE OPA-28 Solution, is above or below the established Minimum Recommended Concentration (MRC) of 0.35%.

Device Description

The device is a qualitative, single use, reagent test strip made up of a 0.40 inch square indicator pad that has been chemically treated to detect OPA. The pad is affixed to one end of a 3.25 inch by 0.40 inch white opaque polystyrene strip.

AI/ML Overview

The SERIM Research Corporation RAPICIDE OPA-28 Test Strip is a chemical indicator designed to determine if the concentration of ortho-phthalaldehyde (OPA), the active ingredient in RAPICIDE OPA-28 Solution, is above or below its established Minimum Recommended Concentration (MRC) of 0.35%.

Here's an analysis of its acceptance criteria and supporting studies:

1. Acceptance Criteria and Reported Device Performance

The provided document indicates the device must reliably indicate if the OPA concentration is above or below the MRC of 0.35%.
The clinical study demonstrated that the device met these criteria through comparative performance with a predicate device.

Acceptance CriteriaReported Device Performance
Reliable indication of OPA concentration (above or below MRC of 0.35% in RAPICIDE OPA-28).The RAPICIDE OPA-28 Test Strips were evaluated in OPA solutions of Rapicide OPA-28 at the MRC and above in blind studies. The performance was found to be substantially equivalent to the predicate device, Serim® DISINTEK™ OPA Test Strips (which measure potency in Cidex OPA solutions at the MEC and above). The study concludes that the test strip is "safe and effective in monitoring the OPA concentration in Rapicide OPA-28 Disinfectant Solution."

2. Sample Size and Data Provenance

The document does not explicitly state the exact sample size (number of test strips or OPA solution samples) used for the blind studies.
The data provenance is not specified regarding country of origin or whether it was retrospective or prospective. Given the nature of a 510(k) submission for a diagnostic device, it is highly likely that the studies were prospective, conducted at the manufacturer's facilities.

3. Number of Experts and Qualifications for Ground Truth

The document does not specify the number of experts used or their qualifications for establishing ground truth. For chemical indicators like this, the "ground truth" would likely be established through analytical chemistry methods (e.g., spectrophotometry or titration) to precisely determine the OPA concentration in the test solutions, rather than human interpretation of the strips themselves as the primary ground truth.

4. Adjudication Method

The document does not describe an adjudication method. For a qualitative chemical indicator where the "ground truth" is a defined chemical concentration, judgment calls by multiple experts with an adjudication method are typically not required. The comparison is against an analytical standard.

5. Multi-Reader Multi-Case (MRMC) Comparative Effectiveness Study

No MRMC comparative effectiveness study was mentioned. This type of study is typically relevant for interpretative devices where human variability in reading results is a significant factor. For a chemical indicator, the reading is expected to be relatively straightforward (color change), reducing the need for such a complex reader study. The study focused on the performance of the device itself rather than human improvement with AI assistance.

6. Standalone Performance Study

Yes, a standalone performance study was done. The "Performance" section explicitly states that "The performance of the RAPICIDE OPA-28 Test Strips was evaluated in OPA solutions of Rapicide OPA-28 at the MRC and above in blind studies." This evaluation determines the device's ability to accurately indicate the OPA concentration without human-in-the-loop assistance in the interpretation of the color change.

7. Type of Ground Truth Used

The ground truth used would be analytical determination of OPA concentration. The study involved evaluating the test strips in "OPA solutions of Rapicide OPA-28 at the MRC and above." This implies that the OPA concentrations in these solutions were precisely known through validated analytical chemistry methods, serving as the objective ground truth against which the test strip's performance was measured.

8. Sample Size for the Training Set

The document does not provide information about a "training set" or its sample size. This is common for chemical indicators of this type, which are typically developed based on chemical principles rather than machine learning algorithms requiring explicit training data. The development process would involve formulation and optimization of the reagents to achieve the desired color change at the target concentration.

9. How Ground Truth for the Training Set Was Established

As there is no mention of a "training set" in the context of machine learning, there is no corresponding ground truth establishment method described. The development of the test strip would rely on chemical formulation and empirical testing against analytically prepared OPA solutions with known concentrations.

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SERIM Research Corporation 510(k) Premarket Notification RAPICIDE OPA-28 Test Strip

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14120652

510(K) SUMMARY

OCT 12 2012

Prepared:February 27, 2012
Submitter:Serim Research Corporation
AddressP.O. Box 4002Elkhart IN 46514
Phone:Fax:574-264-3440574-266-6222
Contact:Patricia A. RupchockDirector of Regulatory Affairs
Device Trade Name:RAPICIDE OPA-28 Test Strips
Common or Usual Name:Indicator for ortho-phthalaldehyde (OPA) high leveldisinfectant
Device Classification Name:Chemical Indicators for Liquid Chemical Germicide. (b)Class II (Physical/Chemical Sterilization ProcessIndicator).
Product Code:JOJ
Class:II
Regulation Number:21CFR 880.2800
Substantial Equivalence:The RAPICIDE OPA-28 Test Strip is substantiallyequivalent to Serim® DISINTEK™ OPA Test Strips, SerimResearch Corporation, P/N 5121; K081370.
Device Description:The device is a qualitative, single use, reagent test stripmade up of a 0.40 inch square indicator pad that has beenchemically treated to detect OPA. The pad is affixed to oneend of a 3.25 inch by 0.40 inch white opaque polystyrenestrip.
Intended Use:The RAPICIDE OPA-28 Test Strip is a chemical indicatorfor use in determining whether the concentration of ortho-phthalaldehyde, the active ingredient in RAPICIDE OPA-28 Solution, is above or below the established MinimumRecommended Concentration (MRC) of 0.35%.

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Technological Characteristics:

The RAPICIDE OPA-28 Test Strip contains two reacting chemicals, a stabilizer, and other non-reacting ingredients. The reaction process involved with the test strip is based on a two step reaction. The first step involves a reaction in which a chemical reacts with the OPA to form a colorless product. A second reaction then occurs in which OPA in excess reacts with a second chemical to form a colored compound, resulting in green color. The test pad size of 0.4" x 0.4" allows for easy interpretation of the change in color. The device will reliably indicate if the OPA concentration-is-above-or-below-the-MRC-of-0.35%-OPA .- -

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Performance:

The performance of the RAPICIDE OPA-28 Test Strips was evaluated in OPA solutions of Rapicide OPA-28 at the MRC and above in blind studies and compared to test results obtained with Serim® DISINTEKTM OPA Test Strips evaluated in Cidex OPA solutions at the MEC and above as well. The performance of the RAPICIDE OPA-28 Test Strips is substantially equivalent to the predicate device, Serim® DISINTEK™ OPA Test Strips.

Summary of Non-clinical Testing

The following table summarizes the non-clinical testing performed to demonstrate that the Rapicide OPA-28 Test strip is safe and effective in monitoring the OPA concentration in Rapicide OPA-28 Disinfectant Solution.

StudyResult
Shelf LifePassed
Open Bottle StabilityPassed
Effect of ContaminantsPassed
Effect of Temperature DeviationPassed
Effect of pH DeviationPassed
Analytical SpecificityPassed

The RAPICIDE OPA-28 Test Strips have the same Conclusion: intended use as the predicate device. Both test strips measure the potency of ortho-phthalaldehyde (OPA) in disinfectant solution, to determine whether it is above or Recommended the Minimum or Effective below Concentration. The difference between the proposed OPA indicator and the predicate device is its use with a different OPA based disinfectant. We are adding a new indication for use to the predicate device, namely the use in the RAPICIDE OPA-28 solution. This difference does not raise any new safety or effectiveness issues.

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DEPARTMENT OF HEALTH & HUMAN SERVICES

Image /page/2/Picture/1 description: The image shows the logo for the U.S. Department of Health & Human Services. The logo features a stylized eagle with its wings spread, and the words "DEPARTMENT OF HEALTH & HUMAN SERVICES • USA" are arranged in a circular pattern around the eagle. The logo is black and white.

Public Health Service

Food and Drug Administration 10903 New Hampshire Avenue Document Control Room -WO66-G609 Silver Spring, MD 20993-0002

OCT 12 2012

Serim Research Corporation Ms. Patricia Rupchock Director of Regulatory Affairs 3506 Reedy Drive Elkhart, Indiana 46514

Re: K120652

Trade/Device Name: Rapicide OPA-28 Test Strips Regulation Number: 21 CFR 880.2800 Regulation Name: Sterilization Process Indicator Regulatory Class: II Product Code: JOJ Dated: October 2, 2012 Received: October 4, 2012

Dear Ms. Rupchock:

We have reviewed your Section 510(k) premarket notification of intent to market the device referenced above and have determined the device is substantially equivalent (for the indications for use stated in the enclosure) to legally marketed predicate devices marketed in interstate commerce prior to May 28, 1976, the enactment date of the Medical Device Amendments, or to devices that have been reclassified in accordance with the provisions of the Federal Food, Drug, and Cosmetic Act (Act) that do not require approval of a premarket approval application (PMA). You may, therefore, market the device, subject to the general controls provisions of the Act. The general controls provisions of the Act include requirements for annual registration, listing of devices, good manufacturing practice, labeling, and prohibitions against misbranding and adulteration. Please note: CDRH does not evaluate information related to contract liability warranties. We remind you, however, that device labeling must be truthful and not misleading.

If your device is classified (see above) into either class II (Special Controls) or class III (PMA), it may be subject to additional controls. Existing major regulations affecting your device can be found in the Code of Federal Regulations, Title 21, Parts 800 to 898. In addition, FDA may publish further announcements concerning your device in the Federal Register.

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Page 2- Ms. Rupchock

Please be advised that FDA's issuance of a substantial equivalence determination does not mean that FDA has made a determination that your device complies with other requirements of the Act or any Federal statutes and regulations administered by other Federal agencies. You must comply with all the Act's requirements, including, but not limited to: registration and listing (21 CFR Part 807); labeling (21 CFR Part 801); medical device reporting (reporting of medical device-related adverse events) (21 CFR 803); good manufacturing practice requirements as set forth in the quality systems (QS) regulation (21 CFR Part 820); and if applicable, the electronic product radiation control provisions (Sections 531-542 of the Act); 21 CFR 1000-1050.

If you desire specific advice for your device on our labeling regulation (21 CFR Part 801), please go to

http://www.fda.gov/AboutFDA/CentersOffices/CDRH/CDRHOffices/ucm115809.htm for the Center for Devices and Radiological Health's (CDRH's) Office of Compliance. Also, please note the regulation entitled, "Misbranding by reference to premarket notification" (21CFR Part 807.97). For questions regarding the reporting of adverse events under the MDR regulation (21 CFR Part 803), please go to

http://www.fda.gov/MedicalDevices/Safety/ReportaProblem/default.htm for the CDRH's Office of Surveillance and Biometrics/Division of Postmarket Surveillance.

You may obtain other general information on your responsibilities under the Act from the Division of Small Manufacturers, International and Consumer Assistance at its toll-free number (800) 638-2041 or (301) 796-7100 or at its Internet address http://www.fda.gov/MedicalDevices/Resourcesfor You/Industry/default.htm.

Sincerely yours,

For

Anthony D. Watson, B.S., M.S., M.B.A. Director Division of Anesthesiology, General Hospital, Infection Control and Dental Devices Office of Device Evaluation Center for Devices and

Radiological Health

Enclosure

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K12 0652

CONFIDENTIAL

SERIM Research Corporation 510(k) Premarket Notification RAPICIDE OPA-28 Test Strip

INDICATIONS FOR USE

510(k) Number (if known): K

RAPICIDE OPA-28 Test Strips Device Name:

Indications For Use: The RAPICIDE OPA-28 Test Strip is a chemical indicator for use in determining whether the ... the ... concentration of ortho-phthalaldehyde, the active ingredient in RAPICIDE OPA-28 Solution, is above or below the established Minimum Recommended Concentration (MRC) of 0.35%.

Prescription Use (Part 21 CFR 801 Subpart D) AND / OR

Over-The-Counter Use (21 CFR 801 Subpart C)

(PLEASE DO NOT WRITE BELOW THIS LINE-CONTINUE ON ANOTHER PAGE IF NEEDED)

Concurrence of CDRH, Office of Device Evaluation (ODE)

Elizabeth F. Clamton Will

(Division Sign-Off) Division of Anesthesiology, General Hospital Infection Control, Dental Devices

510(k) Number:

§ 880.2800 Sterilization process indicator.

(a)
Biological sterilization process indicator —(1)Identification. A biological sterilization process indicator is a device intended for use by a health care provider to accompany products being sterilized through a sterilization procedure and to monitor adequacy of sterilization. The device consists of a known number of microorganisms, of known resistance to the mode of sterilization, in or on a carrier and enclosed in a protective package. Subsequent growth or failure of the microorganisms to grow under suitable conditions indicates the adequacy of sterilization.(2)
Classification. Class II (performance standards).(b)
Physical/chemical sterilization process indicator —(1)Identification. A physical/chemical sterilization process indicator is a device intended for use by a health care provider to accompany products being sterilized through a sterilization procedure and to monitor one or more parameters of the sterilization process. The adequacy of the sterilization conditions as measured by these parameters is indicated by a visible change in the device.(2)
Classification. Class II (performance standards).